Volume 4, Issue 1 (6-2022)
pbp 2022, 4(1): 49-53 |
Back to browse issues page
Download citation:
BibTeX | RIS | EndNote | Medlars | ProCite | Reference Manager | RefWorks
Send citation to:
BibTeX | RIS | EndNote | Medlars | ProCite | Reference Manager | RefWorks
Send citation to:
Ur Rehman I, Malik L, Zaheer S, Abdullah M. A Brief Study of Mass Spectrometry of Natural Products. pbp 2022; 4 (1) :49-53
URL: http://pbp.medilam.ac.ir/article-1-89-en.html
URL: http://pbp.medilam.ac.ir/article-1-89-en.html
1- The University Of Lahore, Sargodha , inshaurrehman82@gmail.com
2- The University Of Lahore, Sargodha
2- The University Of Lahore, Sargodha
Abstract: (2771 Views)
Objective: The physical and chemical data of the pure substance can be analysed to determine the structure. In the current era of structural elucidation, NMR spectroscopy and mass spectroscopy, especially the various types of 2D NMR, are used extensively, while infrared (IR) and ultraviolet spectroscopy (UV) are main tool to recognize the functional groups in the structure. The correlation of key chemicals in chromatograph peaks with individual mass spectra is commonly accomplished using HPLC mass spectrometry (LCMS). For most chemicals studied, LCMS ionisation procedures are chemically mild, and strong molecular ion peaks are detected. MS (mass spectrometry) is a technique for determining a substance's molecular mass, formula, and fragmentation pattern. The most widely deployed techniques in mass spectrometry are electrospray ionisation mass spectrometry, chemical ionization mass spectrometry, chemical ionisation mass spectrometry, and fast atom bombardment mass spectrometry. Our paper discusses in brief how mass spectrometry can be used to study and analyze natural products in a scientific manner. Mass spectrometry, which has been used to study complex biological systems for more than a century, is currently at a critical crossroads. We'll be looking at how the mass spectrometry business is expected to change over the next decade, emphasising the natural products industry's increasing techniques and technology. This research aims to provide a fast summary of how mass spectrometry is used in many disciplines.
Material and Methods: This review study relies on three search engines, Pub Med, Science Direct, Google Scholar, and printed material from the library, to do the best literature research possible.
Conclusion: We highlight growing mass spectrometric methodologies and technologies employed by the natural product field in this viewpoint piece and provide a glimpse into the future directions in which the mass spectrometry field will migrate over the next decade.
Material and Methods: This review study relies on three search engines, Pub Med, Science Direct, Google Scholar, and printed material from the library, to do the best literature research possible.
Conclusion: We highlight growing mass spectrometric methodologies and technologies employed by the natural product field in this viewpoint piece and provide a glimpse into the future directions in which the mass spectrometry field will migrate over the next decade.
Type of Study: Review/Systemtic review |
Subject:
Phytochemistry
Received: 2022/03/21 | Accepted: 2022/04/17 | Published: 2022/04/17
Received: 2022/03/21 | Accepted: 2022/04/17 | Published: 2022/04/17
References
1. Bouslimani A, Sanchez LM, Garg N, Dorrestein PC. Mass spectrometry of natural products: current, emerging and future technologies. Natural Prod Rep 2014; 31(6) 718-729.
2. Esquenazi E, Yang YL, Watrous J, Gerwick WH, Dorrestein PC. Imaging mass spectrometry of natural products. Nat Prod Rep 2009; 26(12) 1521-1534.
3. Xing J, Xie C, Lou H. Recent applications of liquid chromatography– mass spectrometry in natural products bioanalysis. J Pharmac Biomed Anal 2007; 44(2) 368-378.
4. Al-Rubaye AF, Hameed IH, Kadhim MJ. A review: uses of gas chromatography-mass spectrometry (GC-MS) technique for analysis of bioactive natural compounds of some plants. Int J Toxicol Pharmacol Res 2017; 9(1): 81-85.
5. Demarque DP, Crotti AE, Vessecchi R, Lopes JL, Lopes NP. Fragmentation reactions using electrospray ionization mass spectrometry: an important tool for the structural elucidation and characterization of synthetic and natural products. Natural Prod Rep 2016;33(3) 432-455.
6. Alvarez G, Ballesteros D, Parada F, Ibanez E, Cifuentes A. Recent applications of high resolution mass spectrometry for the characterization of plant natural products. TrAC Trends Analyt Chem 2019; 112, 87-101.
7. Noriega P, Ballesteros J, De la Cruz A, Veloz T. Chemical composition and preliminary antimicrobial activity of the hydroxylated sesquiterpenes in the essential oil from Piper barbatum Kunth leaves. Plants 2020; 9(2) 211.
8. Valarezo E, Merino G, Cruz-Erazo C, Cartuche L. Bioactivity evaluation of the native Amazonian species of Ecuador: Piper lineatum Ruiz & Pav. Essential oil. Natural Volatiles Essen Oils 2020; 7(4) 14-25.
9. Adams RP. Identification of essential oils by ion trap mass spectroscopy. Academic press; 2012.
10. Noriega P, Mosquera T, Paredes E, Parra M, Zappia M, Herrera M, Osorio E. Antimicrobial and antioxidant bioautography activity of bark essential oil from Ocotea quixos (Lam.) kosterm. JPC-Journal of Planar Chromatography- Modern TLC 2018; 31(2) 163-168.
11. Koria L, Nithya G. Analysis of Daturastramonium Linn. biodiesel by gas chromatography-mass spectrometry. J Phytochem 4(1); https://updatepublishing.com/journal/index.php/jp/article/view/2751
12. Liu Z, Ezernieks V, Rochfort S, Cocks B. Comparison of methylation methods for fatty acid analysis of milk fat. Food Chem 2018; 261, 210-215.
13. Xia W, Budge SM. GC-MS Characterization of Hydroxy Fatty Acids Generated From Lipid Oxidation in Vegetable Oils. Europ J Lipid Sci Technol 2018; 120(2) 1700313.
14. Benítez R, Coronell C, Martin J. Chemical Characterizaction Sacha Inchi (Plukenetia Volubilis) Seed: Oleaginosa Promising From the Colombian Amazon. Int J Curr Sci Res Rev 2018; 1(1) 1-12.
15. Wannes WA, Mhamdi B, Saidani TM, Marzouk B. Lipid and volatile composition of borage (Borago officinalis L.) leaf. Trends Phytochemical Res 2017; 1(3)143-148.
16. Yi T, Li SM, Fan JY, Fan LL, Zhang ZF, Luo P, Chen HB. Comparativeanalysis of EPA and DHA in fish oil nutritional capsules by GC-MS. Lipids Health Dis 2014; 13(1) 1-6.
17. Song J, Gardner BD, Holland JF, Beaudry RM. Rapid analysis of volatile flavor compounds in apple fruit using SPME and GC/time-of-flight mass spectrometry. J Agricultural Food Chem1997; 45(5) 1801-1807.
18. Noriega P, Calero D, Larenas C, Maldonado ME, Vita FP. Componentes volátiles de los frutos de Vasconcellea pubescens A. DC. y Passiflora tripartite var. mollissima (Kunth) usando la metodologia HS-SPME-GC/MS. La Granja 2014; 19(1).
19. Proestos C, Komaitis M. Analysis of naturally occurring phenolic compounds in aromatic plants by RP-HPLC coupled to diode array detector (DAD) and GC-MS after silylation. Foods 2013; 2(1) 90-99.
20. Proestos C, Komaitis M. Analysis of naturally occurring phenolic compounds in aromatic plants by RP-HPLC coupled to diode array detector (DAD) and GC-MS after silylation. Foods 2013; 2(1) 90-99.
21. Proestos C, Kapsokefalou M, Komaitis M. Analysis of naturally occurring phenolic compounds in aromatic plants by RP-HPLC and GC-MS after silylation. J Food Quality 2018; 31(3) 402-414.
22. Seeram NP, Lee R, Scheuller HS, Heber D. Identification of phenolic compounds in strawberries by liquid chromatography electrospray ionization mass spectroscopy. Food Chem 2006;97(1) 1-11
23. Zeng G, Xiao H, Liu J, Liang X. Identification of phenolic constituents in Radix Salvia miltiorrhizae by liquid chromatography/electrospray ionization mass spectrometry. Rapid Communs Mass Spectr 2006; 20(3) 499-506.
24. Wolfender JL, Waridel P, Ndjoko K, Hobby KR, Major HJ, Hostettmann K. Evaluation of Q-TOF-MS/MS and multiple stage IT-MSn for the dereplication of flavonoids and related compounds in crude plant extracts. Analusis 2000; 28(10) 895-906.
25. Lv Z, Dong J, Zhang B. Rapid identification and detection of flavonoids compounds from bamboo leaves by LC-(ESI)-IT-TOF/MS. BioRes 2012;7(2) 1405-1418.
26. Dias AL, Rozet E, Larondelle Y, Hubert P, Rogez H, Quetin-Leclercq J. Development and validation of an UHPLC-LTQ-Orbitrap MS method for non-anthocyanin flavonoids quantification in Euterpe oleracea juice. Analytical Bioanalytical Chem 2013; 405(28) 9235-9249.
27. Lisko JG, Stanfill SB, Duncan BW, Watson CH. Application of GC-MS/MS for the analysis of tobacco alkaloids in cigarette filler and various tobacco species. Analytical Chem 2013; 85(6) 3380-3384.
28. Amini T, Hashemi P. Preconcentration and GC–MS determination of caffeine in tea and coffee using homogeneous liquid–liquid microextraction based on solvents volume ratio alteration. J Chromatography B 2018; 1092 252-257.
29. González J, Monan M, Perez J, Gómez E, Salgado DDLC, Pérez D. Determination of Theobromine and Caffeine in Theobroma cacao Husk from Ethanolic Extract by GC-MS after CC Separation. Open Access Library J 2019;6(11) 1-9.
30. Namera A, Yashiki M, Hirose Y, Yamaji S, Tani T, Kojima T. Quantitative analysis of tropane alkaloids in biological materials by gas chromatography–mass spectrometry. Forensic Sci Int 2002;130(1) 34-43.
31. Beales KA, Betteridge K, Colegate SM, Edgar JA. Solid-phase extraction and LC− MS analysis of pyrrolizidine alkaloids in honeys. J Agricultural Food Chem 2004; 52(21) 6664-6672.
32. Ding B, Zhou T, Fan G, Hong Z, Wu Y. Qualitative and quantitative determination of ten alkaloids in traditional Chinese medicine Corydalis yanhusuo WT Wang by LC–MS/MS and LC–DAD. J Pharmaceutical Biomedical Analysis 2007;45(2) 219-226.
33. Avula B, Wang YH, Wang M, Smillie TJ, Khan IA. Simultaneous determination of sesquiterpenes and pyrrolizidine alkaloids from the rhizomes of Petasites hybridus (L.) GMet Sch. and dietary supplements using UPLC-UV and HPLC-TOF-MS methods. J Pharmac Biomed Analy 2012; 70 53-63.
34. Pan H, Yang W, Zhang Y, Yang M, Feng R, Wu W, Guo D. An integrated strategy for the systematic characterization and discovery of new indole alkaloids from Uncaria rhynchophylla by UHPLC/DAD/LTQOrbitrap-MS. Analytical Bioanalytical Chem 2015; 407(20) 6057-6070.
35. Delmas MD, Hereu DC. Uso terapéutico de los cannabinoides. Adicciones. 2004; 16(2) 143-152.
36. Grotenhermen F. Los cannabinoidesy el sistema endocannabinoide. Cannabinoids 2006; 1(1) 10-14.
37. Jang E, Kim H, Jang S, Lee J, Baeck S, In S, Han E. Concentrations of THC, CBD, and CBN in commercial hemp seeds and hempseed oil sold in Korea. Forensic Sci Int 2020; 306, 110064.
38. Kintz P, Cirimele V. Testing human blood for cannabis by GC–MS. Biomed Chromatography 1997; 11(6) 371-373.
39. Berman P, Futoran K, Lewitus GM, Mukha D, Benami M, Shlomi T, Meiri D. A new ESI-LC/MS approach for comprehensive metabolic profiling of phytocannabinoids in Cannabis, Sci Rep 2018; 8(1) 1-15.
40. Palazzoli F, Citti C, Licata M, Vilella A, Manca L, Zoli M, Cannazza G. Development of a simple and sensitive liquid chromatography triple quadrupole mass spectrometry (LC–MS/MS) method for the determination of cannabidiol (CBD), Δ9- tetrahydrocannabinol (THC) and its metabolites in rat whole blood after oral administration of a single high dose of CBD. J Pharmac Biomed Analysis 2018; 150 25-32.
Send email to the article author
| Rights and permissions | |
 |
This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License. |